HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Dichloroaniline → HCID 71179006, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Dichloroaniline | HCID 7262 | — |
| Reactant | HCID 178469627 | HCID 178469627 | — |
| Product | HCID 71179006 | HCID 71179006 | 75.5% |
Reaction Steps
Using ethyl 7-hydroxypyrazolo[1,5-a]pyrimidine-6-carboxylate (7.50 g, 36.2 mmol) and 2,5-dichloroaniline (5.30 g, 32.6 mmol) instead of 4-fluoro-2-methylaniline, and in the same manner as in Example 1 step 1, the title compound (8.64 g, 68%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-de32a61486da4cfd8782ba45d1880446 |
| Source note | uspto-grants-2014_08 |