HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,5-Difluoroaniline → HCID 71178882, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,5-Difluoroaniline | HCID 67775 | — |
| Reactant | HCID 178469627 | HCID 178469627 | — |
| Product | HCID 71178882 | HCID 71178882 | 62.2% |
Reaction Steps
Using ethyl 7-hydroxypyrazolo[1,5-a]pyrimidine-6-carboxylate (2.0 g, 9.65 mmol) and 2,5-difluoroaniline (1.12 g, 8.69 mmol) instead of 4-fluoro-2-methylaniline, and in the same manner as in Example 1 step 1, the title compound (1.72 g, 56%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-9a54a134f9714e75807145d53d35eeb8 |
| Source note | uspto-grants-2014_08 |