HuagongsheHuagongshe Chemistry Print Report · For research reference only
3,4-Dichloroaniline → HCID 71179069, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3,4-Dichloroaniline | HCID 7257 | — |
| Reactant | HCID 178469627 | HCID 178469627 | — |
| Product | HCID 71179069 | HCID 71179069 | 71.2% |
Reaction Steps
Using ethyl 7-hydroxypyrazolo[1,5-a]pyrimidine-6-carboxylate (3.0 g, 14.5 mmol) and 3,4-dichloroaniline (1.88 g, 11.6 mmol) instead of 4-fluoro-2-methylaniline, and in the same manner as in Example 1 step 1, the title compound (2.90 g, 57%) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815874B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-3db03c3c1b8549b4a812359579b419ed |
| Source note | uspto-grants-2014_08 |