1,4-Dioxane hydrochloride → HCID 67381180, compound

Participants

Reaction Steps

The compound (7.5 mg, 0.027 mmol) prepared in step 4 was dissolved in 1,4-dioxane (1 ml), added with 3.7 N hydrochloric acid 1,4-dioxane solution (1 ml), and then stirred for 18 hours at room temperature. Once the reaction was completed, generated solid was filtered, washed with ethyl acetate, and dried in vacuo to obtain the title compound (4.5 mg, yield: 25%, white solid).

Provenance & Evidence