Boron tribromide dichloromethane → HCID 58424936, compound

Participants

Reaction Steps

The compound (190 mg, 0.84 mmol) prepared in step 1 was dissolved in dichloromethane (2 ml), added with 1 M boron tribromide dichloromethane solution (4.2 ml). The mixture was stirred overnight at room temperature. The reaction mixture was poured into ice water and the precipitate was collected by filteration to obtain the title compound (125 mg, yield: 70%, yellow solid).

Provenance & Evidence