HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 58424971, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 58424876 | HCID 58424876 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 58424971 | HCID 58424971 | 108.8% |
Reaction Steps
The compound (110 mg, 0.28 mmol) prepared in step 3 was dissolved in 1,4-dioxane, added with 3.7 N hydrochloric acid 1,4-dioxane solution. The resulting mixture was stirred overnight at room temperature and the precipitate was collected by filtration to obtain the title compound (90 mg, yield: 98%, yellow solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815891B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-83092cc34e9247f880f8293303accdfb |
| Source note | uspto-grants-2014_08 |