HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Dioxane hydrochloride → HCID 67381269, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Dioxane hydrochloride | HCID 20443148 | — |
| Reactant | HCID 58424850 | HCID 58424850 | — |
| Solvent | 1,4-Dioxane | HCID 31275 | — |
| Product | HCID 67381269 | HCID 67381269 | 79% |
Reaction Steps
The compound (25 mg, 0.08 mmol) prepared in step 1 was dissolved in 1,4-dioxane (3 ml), added with 3.7 N hydrochloric acid 1,4-dioxane solution. The resulting mixture was stirred for 3 days at room temperature and the precipitate was collected by filtration to obtain the title compound (524 mg, yield: 79%, yellow solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815891B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-b9608b457aff449fa6735cc95b2d4f37 |
| Source note | uspto-grants-2014_08 |