1,4-Dioxane hydrochloride → HCID 58424899, compound

Participants

Reaction Steps

The compound (580 mg, 1.627 mmol) prepared in step 4 was dissolved in 1,4-dioxane (10 ml), added with 3.7 N hydrochloric acid 1,4-dioxane solution (6 ml). The resulting mixture was stirred for one day at room temperature and the precipitate was collected by filtration to obtain the title compound (410 mg, yield: 98%, yellow solid).

Provenance & Evidence