Hydrochloric Acid → HCID 67410395, compound

Participants

Reaction Conditions

Reaction Steps

The compound (40 mg, 0.120 mmol) prepared in step 7 was dissolved in ethanol (3 ml), added with 12 N hydrochloric acid (2 ml). The resulting mixture was refluxed for 12 hours at 90° C. Once the reaction was completed, the mixture was concentrated under reduced pressure and the residue was washed ethyl acetate to obtain the title compound (36 mg, yield: 84%, yellow solid).

Provenance & Evidence