Hydrochloric Acid → HCID 67381332, compound

Participants

Reaction Conditions

Reaction Steps

The compound (20 mg, 0.06 mmol) prepared in step 7 was dissolved in ethanol (4 ml) and added with conc. hydrochloric acid (0.5 ml). The resulting mixture was stirred for 8 hours at 80° C. and cooled to room temperature. The mixture was then concentrated under reduced pressure to obtain the title compound (18 mg, yield: 82%, yellow solid).

Provenance & Evidence