Hydrochloric Acid → HCID 67381244, compound

Participants

Reaction Steps

The compound (112 mg, 0.34 mmol) prepared in step 9 was dissolved in ethanol (3 ml) and added with 12 N hydrochloric acid (2 ml). The resulting mixture was refluxed for 12 hours. Once the reaction was completed, the mixture was concentrated and recrystallized from methanol/ethyl acetate to obtain the title compound (110 mg, yield: 90%, yellow solid).

Provenance & Evidence