Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 67381302 | HCID 67381302 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67381404 | HCID 67381404 | 92% |
Reaction Steps
The compound (100 mg, 0.34 mmol) prepared in step 3 was dissolved in ethanol (5 ml) and added with conc. hydrochloric acid (1.0 ml). The mixture was stirred overnight at 80° C., cooled to room temperature, and concentrated under reduced pressure to obtain the title compound (89.6 mg, yield: 92%, yellow solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08815891B2 |
|---|
| Source dataset | uspto-grants-2014_08 |
|---|
| ORD ID | ord-2dfb274999c048f090da80b96dfd2f3c |
|---|
| Source note | uspto-grants-2014_08 |
|---|