Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | HCID 58424894 | HCID 58424894 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 67381459 | HCID 67381459 | 86% |
Reaction Steps
The compound (15 mg, 0.05 mmol) prepared in step 6 was dissolved in ethanol (4 ml) and added with conc. hydrochloric acid (0.5 ml). The mixture was stirred overnight at 80° C. and the precipitate was collected by filteration to obtain the title compound (14 mg, yield: 86%, yellow solid).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US08815891B2 |
|---|
| Source dataset | uspto-grants-2014_08 |
|---|
| ORD ID | ord-c5484744c64f4c8ea8d131bcb40da1ee |
|---|
| Source note | uspto-grants-2014_08 |
|---|
