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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2409600Generated: October 30, 2026

HCID 70348174, compound → HCID 68106252, compound

https://huagongshe.com/reaction/2409600

Reaction equation

Participants

RoleNameHCIDCharge
ReactantHCID 70348174HCID 70348174—
CatalystHCID 178418390HCID 178418390—
SolventMethanolHCID 887—
ProductHCID 68106252HCID 6810625299.2%

Reaction Steps

Benzyl[(3-hydroxypyrrolidin-1-yl)sulfonyl]carbamate (2.55 g) was added to MeOH, and subsequently, 10% palladium carbon (657 mg, 55% wet) was added thereto, followed by stirring at a normal temperature/a normal pressure for about 3 hours under a hydrogen atmosphere. The catalyst was collected by filtration through Celite, and the filtrate was concentrated under reduced pressure to obtain 3-hydroxypyrrolidin-1-sulfonamide (1.4 g) as a colorless oily substance.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08815920B2
Source datasetuspto-grants-2014_08
ORD IDord-c205ccf1031f456ebf24e3a6db335a27
Source noteuspto-grants-2014_08