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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 2409788Generated: November 2, 2026

Dimethylamine, hydrochloride → HCID 178493497, compound

https://huagongshe.com/reaction/2409788

Reaction equation

Participants

RoleNameHCIDCharge
ReactantDimethylamine, hydrochlorideHCID 10473—
ReactantHCID 178493498HCID 178493498—
SolventDichloromethane methanolHCID 21226129—
ProductHCID 178493497HCID 178493497—

Reaction Steps

The title compound was prepared in analogy to the procedure described in Example 180 but using dimethylamine hydrochloride (1.5 equiv) instead of N,N,N′-trimethylethylenediamine and 8-(2,6-difluoro-3,5-dimethoxy-phenyl)-quinoxaline-5-carboxylic acid (4-formyl-1H-imidazol-2-yl)-amide (Example 7). Title compound: ES-MS: 469 [M+H]+; tR=3.14 min (System 1); TLC: Rf=0.22 (DCM/MeOH/NH3aq, 91.5:7.5:1).

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS08815901B2
Source datasetuspto-grants-2014_08
ORD IDord-85f994ebee054378a9979b5f924b7b76
Source noteuspto-grants-2014_08