HuagongsheHuagongshe Chemistry Print Report · For research reference only
N-Iodosuccinimide → Methyl 2-amino-5-iodo-4-methoxybenzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | N-Iodosuccinimide | HCID 120273 | — |
| Reactant | Methyl 2-amino-4-methoxybenzoate | HCID 12919999 | — |
| Product | Methyl 2-amino-5-iodo-4-methoxybenzoate | HCID 66820461 | — |
Reaction Steps
Synthesized according to the method of reagent preparation 1 by N-iodosuccinimide iodination of methyl 2-amino-4-methoxybenzoate to give methyl 5-iodo-2-amino-4-methoxybenzoate then proceeding with step 1. 1H NMR (400 MHz, CDCl3): 8.97, (s, 1H), 8.75, 7.31 (s, 1H), 4.08 (s, 3H). GC-MS for C9H6ClIN2O: 319 (M+).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648066B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-ddaadf64dc0a43839c37f76439ae3ae0 |
| Source note | uspto-grants-2014_02 |