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HRID2410099

反应详情

EQUATION

反应方程式

HRID 2410099 的结构方程式

REACTANTS

反应物

2
结构：Cc1ccc(Cl)cc1N
HCID7260

5-Chloro-2-methylaniline

C7H8ClN

结构：CCOC(=O)c1nc(Br)n(C(C)C)c1C(O)c1ccc(C#N)cc1
HCID86707757

未命名化合物

PRODUCTS

生成物

1
结构：CCOC(=O)c1nc(Br)n(C(C)C)c1C(Nc1cc(Cl)ccc1C)c1ccc(C#N)cc1
HCID86707756

未命名化合物

AUXILIARIES

试剂、催化剂与溶剂

1
结构：CCCCCC.CCOC(C)=O
溶剂HCID21226206

未命名化合物

PROCEDURE

实验过程

The title compound was prepared in analogy to the procedure described for step E2 using 2-bromo-5-[(4-cyano-phenyl)-hydroxy-methyl]-1-isopropyl-1H-imidazole-4-carboxylic acid ethyl ester (step H3) and 5-chloro-2-methyl-aniline as starting materials. tR: 1.35 min (LC-MS 2); ESI-MS: 515.2 [M−H]+ (LC-MS 2); Rf=0.16 (hexane/ EtOAc, 3:1).