HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → HCID 86707781, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 4-Borono-3-methoxybenzoic acid | HCID 23134276 | — |
| Product | HCID 86707781 | HCID 86707781 | — |
Reaction Steps
The title compound was prepared in analogy to the procedure described for Intermediate K from 4-carboxy-2-methoxyphenyl boronic acid and ethanolamine. The solvent was removed and then water and EtOAc were added. The phases were separated and the aqueous one was extracted twice with EtOAc. The organics extracts were combined and dried (Na2SO4), and concentrated. The residue was triturated in acetonitrile to give the title compound. tR: 0.42 min (LC-MS 2); ESI-MS: 240.1 [M+H]+ (LC-MS 2).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815926B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-fe38c3c817f04c1e98407f973538d2a7 |
| Source note | uspto-grants-2014_08 |