Hydrochloric Acid → HCID 69316976, compound

Participants

Reaction Steps

To a flask containing tert-butyl 4-{[(4-isobutyoxy-1,2-benzisoxazol-3-yl)oxy]methyl}piperidine-1-carboxylate (98.2 mg, 0.24 mmol, EXAMPLE 1, step 3) was added 4N solution of hydrogen chloride in ethyl acetate (1 mL) at room temperature. After being stirred for 2 h, solvent was evaporated and the residual solid was washed with ethyl acetate to give the title compound (62.4 mg, 75%) as a white solid.

Provenance & Evidence