HCID 58437037, compound → HCID 58437038, compound

Participants

Reaction Steps

Prepared in the same manner as (2R,5R)-2-(tert-Butyl)-5-(3-chlorophenyl)-5-heptyl-1,3-dioxolan-4-one using (2S,5R)-2-(tert-Butyl)-5-(3-chlorophenyl)-1,3-dioxolan-4-one. 1H NMR (400 MHz, CDCl3, δ): 0.84 (t, J=7 Hz, 3H), 0.96 (s, 9H), 1.16-1.35 (m, 10H), 1.88-2.06 (m, 2H), 5.35 (s, 1H), 7.26-7.30 (m, 2H), 7.50-7.54 (m, 1H), 7.62-7.63 (m, 1H). 13C NMR (100 MHz, CDCl3, δ): 14.3, 22.8, 23.7, 23.8, 29.2, 29.5, 31.9, 35.2, 38.9, 82.3, 109.1, 123.4, 125.4, 128.3, 129.7, 134.5, 140.5, 173.5.

Provenance & Evidence