HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethanolamine → 5-bromo-N-(2-hydroxyethyl)-2-(methylamino)pyridine-3-sulfonamide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethanolamine | HCID 700 | — |
| Reactant | 5-Bromo-N-methylpyridin-2-amine | HCID 15645663 | — |
| Reactant | 5-Bromo-2-(methylamino)pyridine-3-sulfonyl chloride | HCID 86647821 | — |
| Product | 5-bromo-N-(2-hydroxyethyl)-2-(methylamino)pyridine-3-sulfonamide | HCID 66820561 | — |
Reaction Steps
Prepared according to the methods described in reagent preparation 25 using 5-bromo-2-(methylamino)pyridine-3-sulfonyl chloride (prepared from 5-bromo-N-methylpyridin-2-amine using analogous conditions to those described in WO2008144463) and 2-aminoethanol in step 1.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08648066B2 |
| Source dataset | uspto-grants-2014_02 |
| ORD ID | ord-10afbe0e984e40d791253d8fe910203b |
| Source note | uspto-grants-2014_02 |