HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydroxylamine → tert-butyl N-{4-[amino(hydroxyimino)methyl]benzyl}-N-methylglycinate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydroxylamine | HCID 787 | — |
| Reactant | tert-butyl N-(4-cyanobenzyl)-N-methylglycinate | HCID 66678135 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | tert-butyl N-{4-[amino(hydroxyimino)methyl]benzyl}-N-methylglycinate | HCID 76685327 | — |
Reaction Steps
A 50% aqueous solution of hydroxylamine (13.25 mL, 225 mmol) was added at once into a solution of tert-butyl N-(4-cyanobenzyl)-N-methylglycinate (11.70 g, 45 mmol) in EtOH (75 mL).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08815919B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-b41010fcebc1451f9dfbeda54257b590 |
| Source note | uspto-grants-2014_08 |