1-Methyl-4-piperidone → HCID 66605455, compound

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Reaction Steps

This was similarly prepared 7-amino-2-(3-(trifluoromethyl)phenyl)-5H-pyrido[3,2-b]indole-4-carboxamide and 1-methylpiperidin-4-one. MS (ESI) m/z 468.30 (M+H); HPLC retention time of 1.85 min with Xbridge S10 4.6×50 mm column, 3 min gradient, 0-100% B, 4 mL/min. Solvent A: 95% MeOH—5% H2O—0.1% TFA; Solvent B: 5% MeOH—95% H2O—0.1% TFA.

Provenance & Evidence