2-Bromo-4-methylphenol → 2-Bromo-1-(cyclopropylmethoxy)-4-methylbenzene

反応式

[Br:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[CH:4][C:3]=1[OH:9].Br[CH2:11][CH:12]1[CH2:14][CH2:13]1>>[Br:1][C:2]1[CH:7]=[C:6]([CH3:8])[CH:5]=[CH:4][C:3]=1[O:9][CH2:11][CH:12]1[CH2:14][CH2:13]1

参加物

反応物 2

HCID 231092-Bromo-4-methylphenol

HCID 81503Bromomethylcyclopropane

生成物 1

HCID 435603972-Bromo-1-(cyclopropylmethoxy)-4-methylbenzene

実験手順

Starting from commercially available 2-bromo-4-methyl-phenol and bromomethyl-cyclopropane the title compound is obtained as colorless oil after distillation at 5×10−3 mbar.

出典と根拠

ORDレコード: ord-d6c0f428692b4e7388bc0c2c498f7c88
出典データセット: uspto-grants-2014_08
DOI: 10.6084/m9.figshare.5104873.v1
特許番号: US08816085B2

反応ノート

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