HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → (S)-3-isopropylisothiazolidine 1,1-dioxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | D-Valinol | HCID 6950587 | — |
| Product | (S)-3-isopropylisothiazolidine 1,1-dioxide | HCID 86676751 | — |
Reaction Steps
Using (R)-2-amino-3-methyl-1-butanol (5.0 g) and methanesulfonyl chloride (7.7 mL) and by the reaction and treatment in the same manner as in Preparation Example 1, the title compound (3.48 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-c546fe0dee5b4417bbcf5106f81db01e |
| Source note | uspto-grants-2014_08 |