HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloropropanesulphonyl chloride → 4-(1,1-Dioxo-1lambda6-isothiazolidin-2-yl)-2-methoxybenzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloropropanesulphonyl chloride | HCID 15410 | — |
| Reactant | Methyl 4-amino-o-anisate | HCID 168705 | — |
| Product | 4-(1,1-Dioxo-1lambda6-isothiazolidin-2-yl)-2-methoxybenzoic acid | HCID 71252082 | — |
Reaction Steps
Using methyl 4-amino-2-methoxybenzoate (1.01 g) and 3-chloropropane-1-sulfonyl chloride (0.9 mL) and by the reaction and treatment in the same manner as in Preparation Example 16, the title compound (839 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-4fdd1796336a42e6b75122283533e884 |
| Source note | uspto-grants-2014_08 |