HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloropropanesulphonyl chloride → 2,4-Bis(1,1-dioxo-1lambda6-isothiazolidin-2-yl)benzoic acid
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloropropanesulphonyl chloride | HCID 15410 | — |
| Reactant | Ethyl 2,4-diaminobenzoate | HCID 22096618 | — |
| Product | 2,4-Bis(1,1-dioxo-1lambda6-isothiazolidin-2-yl)benzoic acid | HCID 71252293 | — |
Reaction Steps
Using ethyl 2,4-diaminobenzoate (2.21 g) and 3-chloropropane-1-sulfonyl chloride (4 mL) and by the reaction and treatment in the same manner as in Preparation Example 16, the title compound (1.33 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-306ad5a852224c4b87d88f5c735fa1a6 |
| Source note | uspto-grants-2014_08 |