HuagongsheHuagongshe Chemistry Print Report · For research reference only
3-Chloropropanesulphonyl chloride → Methyl 4-[1-(1,1-dioxo-1lambda6-isothiazolidin-2-yl)-1-methylethyl]benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 3-Chloropropanesulphonyl chloride | HCID 15410 | — |
| Reactant | Methyl 4-(1-amino-1-methylethyl)benzoate | HCID 57572309 | — |
| Product | Methyl 4-[1-(1,1-dioxo-1lambda6-isothiazolidin-2-yl)-1-methylethyl]benzoate | HCID 71252862 | — |
Reaction Steps
Using methyl 4-(1-amino-1-methylethyl)benzoate (570 mg) and 3-chloropropane-1-sulfonyl chloride (0.47 mL) and by the reaction and treatment in the same manner as in Preparation Example 17, the title compound (862 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-56068c774a014b379e91b2179bd9beef |
| Source note | uspto-grants-2014_08 |