HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanesultam → HCID 71252272, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanesultam | HCID 642157 | — |
| Reactant | 6-Bromomethyl-nicotinic acid methyl ester | HCID 12752237 | — |
| Product | HCID 71252272 | HCID 71252272 | 73% |
Reaction Steps
Using methyl 6-bromomethylnicotinate (500 mg) and 1,1-dioxo-1λ6-isothiazolidine (290 mg) and by the reaction and treatment in the same manner as in Preparation Example 42, the title compound (429 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-97a518bed642420eb6262dca1bfbd2f0 |
| Source note | uspto-grants-2014_08 |