HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonyl chloride → methyl (S)-4-(1-methanesulfonylaminoethyl)benzoate
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonyl chloride | HCID 31297 | — |
| Reactant | Methyl 4-((1S)-1-aminoethyl)benzoate | HCID 17751895 | — |
| Product | methyl (S)-4-(1-methanesulfonylaminoethyl)benzoate | HCID 71262918 | — |
Reaction Steps
Using methyl (S)-4-(1-aminoethyl)benzoate (0.61 g) and methanesulfonyl chloride (0.29 mL) and by the reaction and treatment in the same manner as in Preparation Example 71, the title compound (0.81 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-fb924fb53f7e423d92e701fbc088fc69 |
| Source note | uspto-grants-2014_08 |