HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromopyridine-2-carboxylic acid → HCID 71252936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromopyridine-2-carboxylic acid | HCID 608544 | — |
| Reactant | 1-(5-Ethyl-3-methylpyridin-2-yl)piperazine | HCID 58484578 | — |
| Product | HCID 71252936 | HCID 71252936 | 42.8% |
Reaction Steps
Using 5-bromo-2-picolinic acid (206 mg) and 1-(5-ethyl-3-methylpyridin-2-yl)piperazine (220 mg) described in Preparation Example 81 and by the reaction and treatment in the same manner as in Preparation Example 109, the title compound (170 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-5c8cc4b171b54998b951eed6d25fc6d4 |
| Source note | uspto-grants-2014_08 |