HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(5-Bromo-3-methylpyridin-2-yl)piperazine → HCID 58484740, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(5-Bromo-3-methylpyridin-2-yl)piperazine | HCID 46739270 | — |
| Reactant | 6-Fluoro-4-methylpyridine-3-carboxylic acid | HCID 46739274 | — |
| Product | HCID 58484740 | HCID 58484740 | 86.8% |
Reaction Steps
Using 6-fluoro-4-methylnicotinic acid (1.00 g) and 1-(5-bromo-3-methylpyridin-2-yl)piperazine (1.65 g) and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (2.20 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-fab4b36cb0cd42b9b664d2b8db0c9d9a |
| Source note | uspto-grants-2014_08 |