HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromopyridine-2-carboxylic acid → HCID 71251982, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromopyridine-2-carboxylic acid | HCID 608544 | — |
| Reactant | 1-(3,5,6-Trimethylpyridin-2-yl)piperazine | HCID 58484823 | — |
| Product | HCID 71251982 | HCID 71251982 | 63.3% |
Reaction Steps
Using 1-(3,5,6-trimethylpyridin-2-yl)piperazine (1.5 g) described in Preparation Example 92 and 5-bromo-2-picolinic acid (1.5 g) and by the reaction and treatment in the same manner as in Preparation Example 118, the title compound (1.8 g) was obtained
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-a1a4d5369e314ca38a545bb53b0eec6c |
| Source note | uspto-grants-2014_08 |