HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-Fluoro-4-methylpyridine-3-carboxylic acid → HCID 71252523, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-Fluoro-4-methylpyridine-3-carboxylic acid | HCID 46739274 | — |
| Reactant | 1-(3,5,6-Trimethylpyridin-2-yl)piperazine | HCID 58484823 | — |
| Product | HCID 71252523 | HCID 71252523 | 83.8% |
Reaction Steps
Using 6-fluoro-4-methylnicotinic acid (119 mg) and 1-(3,5,6-trimethylpyridin-2-yl)piperazine (170 mg) described in Preparation Example 92 and by the reaction and treatment in the same manner as in Preparation Example 118, the title compound (220 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-e7b0abaab959490494408655ba015c9d |
| Source note | uspto-grants-2014_08 |