HRID2411332

反应详情

EQUATION

反应方程式

REACTANTS

反应物

HCID2771431

1-(3,5-Dichloro-2-pyridyl)piperazine

C9H11Cl2N3

结构：CS(=O)(=O)c1cc(N2CCCS2(=O)=O)ccc1C(=O)O

HCID71252108

未命名化合物

PRODUCTS

生成物

结构：CS(=O)(=O)c1cc(N2CCCS2(=O)=O)ccc1C(=O)N1CCN(c2ncc(Cl)cc2Cl)CC1

HCID71252471

未命名化合物

收率 12.8%

PROCEDURE

实验过程

Using 4-(1,1-dioxo-1λ6-isothiazolidin-2-yl)-2-methanesulfonylbenzoic acid (319 mg) described in Preparation Example 22 and 1-(3,5-dichloropyridin-2-yl)piperazine (232 mg) and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (68 mg) was obtained.