HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromopyrimidine-2-carboxylic acid → HCID 71252096, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromopyrimidine-2-carboxylic acid | HCID 16462970 | — |
| Reactant | 1-(3,5-Dimethylpyridin-2-yl)piperazine | HCID 58484496 | — |
| Product | HCID 71252096 | HCID 71252096 | 71.9% |
Reaction Steps
Using 5-bromopyrimidine-2-carboxylic acid (0.81 g) and 1-(3,5-dimethylpyridin-2-yl)piperazine (0.77 g) described in Preparation Example 79 and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (1.08 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-6497984e53794fdd9f106aa5384166cf |
| Source note | uspto-grants-2014_08 |