HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromopyrazine-2-carboxylic acid → HCID 86676767, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromopyrazine-2-carboxylic acid | HCID 18779790 | — |
| Reactant | 1-(3,5-Dimethylpyridin-2-yl)piperazine | HCID 58484496 | — |
| Product | HCID 86676767 | HCID 86676767 | 69.5% |
Reaction Steps
Using 5-bromopyrazine-2-carboxylic acid (203 mg) and 1-(3,5-dimethylpyridin-2-yl)piperazine (191 mg) described in Preparation Example 79 and by the reaction and treatment in the same manner as in Preparation Example 118, the title compound (261 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-ebbee38ada434d988d5ef2b3a423fe0b |
| Source note | uspto-grants-2014_08 |