HuagongsheHuagongshe Chemistry Print Report · For research reference only
6-chloropyridazine-3-carboxylic Acid → HCID 86676768, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 6-chloropyridazine-3-carboxylic Acid | HCID 6415762 | — |
| Reactant | 1-(5-Cyclopropyl-3-methylpyridin-2-yl)piperazine | HCID 58484718 | — |
| Product | HCID 86676768 | HCID 86676768 | 64.7% |
Reaction Steps
Using 6-chloropyridazine-3-carboxylic acid (1 g) and 1-(5-cyclopropyl-3-methylpyridin-2-yl)piperazine (1.37 g) described in Preparation Example 83 and by the reaction and treatment in the same manner as in Preparation Example 118, the title compound (1.46 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-5fdc8891184d4e0192c625fad05d8381 |
| Source note | uspto-grants-2014_08 |