HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromothiophene-3-carboxylic acid → HCID 71252690, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromothiophene-3-carboxylic acid | HCID 12039978 | — |
| Reactant | 1-(3,5-Dimethylpyridin-2-yl)piperazine | HCID 58484496 | — |
| Product | HCID 71252690 | HCID 71252690 | 76.2% |
Reaction Steps
Using 5-bromothiophene-3-carboxylic acid (500 mg) and 1-(3,5-dimethylpyridin-2-yl)piperazine (462 mg) described in Preparation Example 79 and by the reaction and treatment in the same manner as in Preparation Example 118, the title compound (700 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-5214d9748300452fb47c2cfa6ea70dd0 |
| Source note | uspto-grants-2014_08 |