HuagongsheHuagongshe Chemistry Print Report · For research reference only
4-Bromo-2-cyanobenzoic acid → HCID 71252294, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 4-Bromo-2-cyanobenzoic acid | HCID 58484585 | — |
| Reactant | 1-(3,5-Dicyclopropylpyridin-2-yl)piperazine | HCID 58484701 | — |
| Product | HCID 71252294 | HCID 71252294 | 92.8% |
Reaction Steps
Using 4-bromo-2-cyanobenzoic acid (3.39 g) described in Preparation Example 76 and 1-(3,5-dicyclopropylpyridin-2-yl)piperazine (4.02 g) described in Preparation Example 88 and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (6.28 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-fd861d89ed314b11b3da05938404b7e7 |
| Source note | uspto-grants-2014_08 |