HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,5,6-Trimethylpyridin-2-yl)piperazine → HCID 86676770, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,5,6-Trimethylpyridin-2-yl)piperazine | HCID 58484823 | — |
| Reactant | 6-BroMo-2-Methyl-nicotinic acid | HCID 71691567 | — |
| Product | HCID 86676770 | HCID 86676770 | 57.6% |
Reaction Steps
Using 6-bromo-2-methylnicotinic acid (745 mg) and 1-(3,5,6-trimethylpyridin-2-yl)piperazine (744 mg) described in Preparation Example 92 and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (801 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-bc26cdaed84441f68bcbf6c12ae08ce2 |
| Source note | uspto-grants-2014_08 |