HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(5-Ethyl-3-methylpyridin-2-yl)piperazine → HCID 86676772, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(5-Ethyl-3-methylpyridin-2-yl)piperazine | HCID 58484578 | — |
| Reactant | 6-BroMo-2-Methyl-nicotinic acid | HCID 71691567 | — |
| Product | HCID 86676772 | HCID 86676772 | 55.3% |
Reaction Steps
Using 6-bromo-2-methylnicotinic acid (675 mg) and 1-(5-ethyl-3-methylpyridin-2-yl)piperazine (611 mg) described in Preparation Example 81 and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (664 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-cb5b380073784858b412fff030a14dbb |
| Source note | uspto-grants-2014_08 |