HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,5-Dicyclopropylpyridin-2-yl)piperazine → HCID 86676773, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,5-Dicyclopropylpyridin-2-yl)piperazine | HCID 58484701 | — |
| Reactant | 6-BroMo-2-Methyl-nicotinic acid | HCID 71691567 | — |
| Product | HCID 86676773 | HCID 86676773 | 56.3% |
Reaction Steps
Using 6-bromo-2-methylnicotinic acid (604 mg) and 1-(3,5-dicyclopropylpyridin-2-yl)piperazine (816 mg) described in Preparation Example 88 and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (695 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-6585959be48d431faace28190830358e |
| Source note | uspto-grants-2014_08 |