HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromo-4-chlorobenzoic acid → HCID 71253010, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromo-4-chlorobenzoic acid | HCID 33126 | — |
| Reactant | 1-(3,5,6-Trimethylpyridin-2-yl)piperazine | HCID 58484823 | — |
| Product | HCID 71253010 | HCID 71253010 | 103.3% |
Reaction Steps
Using 2-bromo-4-chlorobenzoic acid (1 g) and 1-(3,5,6-trimethylpyridin-2-yl)piperazine (0.87 g) described in Preparation Example 92 and by the reaction and treatment in the same manner as in Preparation Example 111, the title compound (1.85 g) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-3fa8c7e48c5f4af4b9eed2d203db6d49 |
| Source note | uspto-grants-2014_08 |