HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(2,6-Dimethylpyridin-3-yl)piperazine → HCID 71252314, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(2,6-Dimethylpyridin-3-yl)piperazine | HCID 58484703 | — |
| Reactant | 4-(1,1-Dioxo-1lambda6-isothiazolidin-2-yl)-2-methanesulfonylbenzoic acid | HCID 71252108 | — |
| Product | HCID 71252314 | HCID 71252314 | 35% |
Reaction Steps
Using 4-(1,1-dioxo-1λ6-isothiazolidin-2-yl)-2-methanesulfonylbenzoic acid (189 mg) described in Preparation Example 22 and 1-(2,6-dimethylpyridin-3-yl)piperazine (113 mg) described in Preparation Example 94 and by the reaction and treatment in the same manner as in Example 87, the title compound (102 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-9135a7c6aa1247b2b50c4e9a5c1b255b |
| Source note | uspto-grants-2014_08 |