HuagongsheHuagongshe Chemistry Print Report · For research reference only
1-(3,5,6-Trimethylpyridin-2-yl)piperazine → HCID 71252439, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1-(3,5,6-Trimethylpyridin-2-yl)piperazine | HCID 58484823 | — |
| Reactant | 4-(1,1-Dioxo-1lambda6-isothiazolidin-2-yl)-2-fluorobenzoic acid | HCID 71252861 | — |
| Product | HCID 71252439 | HCID 71252439 | 63.2% |
Reaction Steps
Using 4-(1,1-dioxo-1λ6-isothiazolidin-2-yl)-2-fluorobenzoic acid (259 mg) described in Preparation Example 23 and 1-(3,5,6-trimethylpyridin-2-yl)piperazine (205 mg) described in Preparation Example 92 and by the reaction and treatment in the same manner as in Example 87, the title compound (282 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-b5f0e015c03d4faea90aa30ed10e8ae9 |
| Source note | uspto-grants-2014_08 |