HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanesultam → HCID 71252747, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanesultam | HCID 642157 | — |
| Reactant | HCID 71251979 | HCID 71251979 | — |
| Product | HCID 71252747 | HCID 71252747 | 91.8% |
Reaction Steps
Using 5-bromo-2-[4-(2,4-dimethylphenyl)piperazine-1-carbonyl]benzonitrile (797 mg) described in Preparation Example 188 and isothiazolidine 1,1-dioxide (315 mg) and by the reaction and treatment in the same manner as in Example 262, the title compound (806 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-316c0bfb0ed8407caa7e993c14f1cf37 |
| Source note | uspto-grants-2014_08 |