HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,3-Propanesultam → HCID 71252374, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,3-Propanesultam | HCID 642157 | — |
| Reactant | 1-Acetyl-3-{5-chloro-2-[4-(3,5-dimethylpyridin-2-yl)piperazine-1-carbonyl]phenyl}imidazolidin-2-one | HCID 58484683 | — |
| Product | HCID 71252374 | HCID 71252374 | 28.1% |
Reaction Steps
Using 1-acetyl-3-{5-chloro-2-[4-(3,5-dimethylpyridin-2-yl)piperazine-1-carbonyl]phenyl}imidazolidin-2-one (117 mg) described in Preparation Example 234 and isothiazolidine 1,1-dioxide (47 mg) and by the reaction and treatment in the same manner as in Example 649, the title compound (36 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-8237abfdff73470ba10c5c8cc82039ba |
| Source note | uspto-grants-2014_08 |