HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Butanesultam → HCID 71252008, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Butanesultam | HCID 303508 | — |
| Reactant | [4-(5-Ethyl-3-methylpyridin-2-yl)piperazin-1-yl](4-iodophenyl)methanone | HCID 58484605 | — |
| Product | HCID 71252008 | HCID 71252008 | 58.5% |
Reaction Steps
Using [4-(5-ethyl-3-methylpyridin-2-yl)piperazin-1-yl](4-iodophenyl)methanone (348 mg) described in Preparation Example 133 and [1,2]thiazinane 1,1-dioxide (141 mg) and by the reaction and treatment in the same manner as in Example 262, the title compound (207 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-13684c11031242cca1b59b2ea8fbbf52 |
| Source note | uspto-grants-2014_08 |