HuagongsheHuagongshe Chemistry Print Report · For research reference only
1,4-Butanesultam → HCID 71252924, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 1,4-Butanesultam | HCID 303508 | — |
| Reactant | HCID 71252298 | HCID 71252298 | — |
| Product | HCID 71252924 | HCID 71252924 | 86.6% |
Reaction Steps
Using 5-bromo-2-[4-(5-ethyl-3-methylpyridin-2-yl)piperazine-1-carbonyl]benzonitrile (827 mg) described in Preparation Example 246 and [1,2]thiazinane 1,1-dioxide (351 mg) and by the reaction and treatment in the same manner as in Example 262, the title compound (810 mg) was obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US08816079B2 |
| Source dataset | uspto-grants-2014_08 |
| ORD ID | ord-4c4ddbfffa0d4a9ba4a4b68db59ff1ac |
| Source note | uspto-grants-2014_08 |